Покращення молекулярно-структурних та лінійних/нелінійних оптичних характеристик нанокомпозитних плівок хітозану/діоксиду титану для пакування та оптоелектронних застосувань
Анотація
Поточне дослідження спрямоване на синтез та характеристику нанокомпозитних плівок хітозану та діоксиду титану з точки зору молекулярної структури, теплових та оптичних властивостей для використання в упаковці продуктів та оптоелектронних застосувань. Інфрачервона спектроскопія з перетворенням Фур’є (FTIR) була використана для вивчення взаємодії між TiO2-NPs і хітозаном, і аналіз підтвердив, що TiO2-NPs взаємодіяли з хітозаном і продемонстрували хорошу сумісність. Диференціальна скануюча калориметрія та термогравіметричний аналіз показали, що збільшення концентрації TiO2-NP покращує термічну стабільність нанокомпозитів. Лінійні оптичні властивості в діапазоні UV-Vis (200–800 нм) вимірювали спектрофотометрично. Нижче 400 нм спектри пропускання нанокомпозитів демонструють знижений ступінь прозорості, що вказує на їх здатність повністю блокувати пропускання УФ-світла. Модель Таука була використана для ідентифікації типів електронних переходів у зразках. Модель одного осцилятора була використана для дослідження енергії та параметрів дисперсії. Також були досліджені нелінійно-оптичні властивості. UV-Vis в області (360-410 нм), аналіз показав, що збільшення концентрації TiO2-NPs від 0 до 12 мас.% зменшує край поглинання з 2,716 до 2,043 еВ, зменшує пряме (3,282 до 2,798 еВ) і непрямі (від 2,417 до 1,581 еВ) енергетичні заборонені зони, збільшили енергію Урбаха з 0,692 до 1,295 еВ, зменшили енергію дисперсії з 11,324 до 5,621 еВ, зменшили енергію одного осцилятора з 6,308 до 5,393 еВ і покращили інші лінійні та нелінійні параметри . Результати підтверджують використання нанокомпозитних плівок CS/TiO2 в пакувальній промисловості та різноманітних оптичних застосуваннях.
Завантаження
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