LOW TEMPERATURE DEFORMATION AND STRENGTH OF POLYIMIDE FILMS DUE TO THICKNESS AND DEFORMATION SPEED
Abstract
In work mechanical properties of polyimide films analogue kapton H (manufactures of the People's Republic of China) with different thickness in the temperature interval 77-293 K and deformation speed interval 10-4-10-3 s-1 are carried out. It is established, that the films are in a forced elastic state at both temperatures of deformation. Contributions to total deformation such as elastic, high elastic (reversible at temperature of test and delay) and irreversible components are determined. It is detected, that relaxation processes which are connected with the contribution of elastic delayed deformation and are accompanied with reduction of their length, take course at exposure at a room temperature of samples after destruction or preliminary deformation. Full removal high elastic delayed deformation occurs after heat treatment at 623 K. Sensitivity of a limit of forced elasticity sв and the contribution of elastic deformation which is reversible at test temperature to deformation speed are established. Influence of the scale factor (thickness of a film) on the mechanical characteristics, which are amplified with downturn of temperature is registered.
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References
2. A.David Grove Polyimide x-ray filter substrates optimized for cryogenic temperatures // Proc. SPIE 3766, X-Ray Optics, Instruments, and Missions II, 386 (September 29, 1999); doi:10.1117/12.363653 (http://www.luxel.com).
3. E. Tschegg, K. Humer and H.W. Weber Mechanical properties and fracture behaviour of polyimide (SINTIMID) at cryogenic temperatures // Cryogenics.- 1991.-Vol.31, October.-P.878 – 883.
4. Malay K.Ghosh, K.L.Mittal Polyimides Fundamentals and Applications, Marcel Dekker Inc., New York.-1996.
5. Abraimov V.V., Agashkova N.N., Bone L., Budnyak I.V., Velichko N.I., Krevsun A.V., Kostenko V.I., Lura F., Markus A.M. Kompleksnye issledovaniya fiziko-mechanicheskih svoystv materialov svetopogloshchayushchih pokrytiy kosmicheskih apparatov proektov “Mars-96” I “Regata” pod vozdeystviem factorov kosmicheskogo prostranstva [Complex researches of physico-mechanical properties of materials of light-absorbing coverings of space vehicles of projects «Mars -96» and "Regatta" under influence of space factors ] // Kosmichna nauka i technologiya [Space Science and Technology].-1995.-Vol.1, No.1.- P.57-68 (in Russian).
6. Abraimov V.V., Lototskaya V.A., Saltevskiy G.I., Zaritskiy I.P Investigation of mechanical properties of polyimide materials in the 4.2-300 K temperatures interval // Conference Abstracts of 4th Inter. Conf. "Space technologies; the present and the future", 17-19 April 2013.- Dnepropetrovsk.- Kyiv - P.88.
7. Abraimov V.V., Lototskaya V.A., Zaritskiy I.P. Investigation of peculiarities of mechanical properties of some polymeric materials in the 4.2-300 K temperatures interval // Conference Abstracts of 4th Inter. Conf. “HighMatTech-2013”, 7-11 October 2013.- Kyiv.- Ukraine.- P.278.
8. Soldatov V.P., Kirichenko G.I., Abraimov V.V., Braude I.S., Geidarov V.G. The laws of deformation of an amorphous polyimide (PI) film when it is stretched in the temperature range 1,6-300 K//Low Temperature Physics.-2016.- No.9.–P.1043-1052.
9. Bessonov M.I., Koton M.M., Kudryavtsev V.V., Layus L.A. Polyimidyu – klass termostoykih polymerov [Polyimides – class of heat-resistant polymers].-L.: Nauka.-1984.-328 p. (in Russian).
10. Bartenev G.M., Zuev Yu.S. Prochnost’ I razrushenie vysokoelastichnyh materialov [Strength and rupture of highly elastic materials М.-L: Izd-vo «Himiyu», 1964.- 335 p. (in Russian).
11. Kargin V.A., Slonimskiy G.L. Kratkie ocherki po fiziko-chimii polymerov [Brief sketches in physics & chemistry of polymers].-М.-L: Izd-vo «Himiyu», 1967.- 232 p. (in Russian).
12. Lur’e E.G., Kovriga V.V. K voprosu o edinstve mehanizma deformatsii I camoproizvol’nogo udlineniya jestkotsepnyh polymerov [To a question about unity of the deformation mechanism and spontaneous lengthening of rigidly chain polymers] // Mechanics of polymers.-1977.- No.4.-P.587-593 (in Russian).
13. Lur’e E.G., Kazaryan L.G., Uchastkina E. L., Kovriga V.V. Vlasova K.N., Dobrohotova M.L., Emel’yanova L.N. Struktura polypiromellitimida I ee vliyanie na fisiko-mehanicheskie cvoystva [Structure of polypiromellitimide and its influence on physico- mechanical properties] //Vysokomolekulyarnye coedineniya .-1974.-Vol.(А) XIII. - No.3. - P.603-607 (in Russian).
14. Braude I.S., Gal’tsov N.N., Geidarov V.G., Kirichenko G.I., Abraimov V.V. Effect of deformation and temperature on ordering of polyimide PM-A - molecules. X-ray data // Low Temperature Physics.-2016.- Vol.42. - No.3.- P.204-207.
Citations
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