Production of Magnetic Nanoparticle-Based Ferrites and Comprehensive Characterization of Their Electrical and Magnetic Properties in Colloidal Systems

Keywords: Magnetic nanoparticles, Ferrite dispersions, Colloidal systems, Magnetic fluid, Nanostructured materials, Electrical conductivity, Magnetic susceptibility

Abstract

This study investigates the synthesis, structural characterization, and physicochemical properties of magnetic nanoparticles derived from iron group metals (Fe, Co, Ni) and their corresponding ferrite dispersions. Magnetic nanoparticles were synthesized via chemical condensation, and their morphology and structure were analyzed using transmission electron microscopy (TEM) and X-ray diffraction (XRD). The synthesized magnetic nanoparticles, comprising Fe3O4, CoFe2O4, and NiFe2O4 ferrites, exhibited nano-scale dimensions ranging from 10 to 50 nm. The precise correlation between TEM and XRD measurements validated the structural and dimensional characteristics of the synthesized nanoparticles. Aqueous-based magnetic liquids with varying nanoparticle concentrations were prepared, enabling systematic investigation of their electrical conductivity and magnetic susceptibility at ambient temperature. The experimental findings provide critical insights into the fundamental properties of magnetic nanoparticle-based colloidal systems, potentially facilitating advanced applications in materials science, magnetic device engineering, and emerging technological domains. The methodological approach and results presented herein contribute to the expanding understanding of magnetic fluid behavior and performance.

Downloads

Download data is not yet available.

References

A.-H. Lu, E.L. Salabas, and F. Schüth, “Magnetic Nanoparticles: Synthesis, Protection, Functionalization, and Application,” Angew. Chem. Int. Ed. 46, 1222–1244 (2007). https://doi.org/10.1002/anie.200602866

S. Laurent, D. Forge, M. Port, A. Roch, C. Robic, L. Vander Elst, and R.N. Muller, “Magnetic Iron Oxide Nanoparticles: Synthesis, Stabilization, Vectorization, Physicochemical Characterizations, and Biological Applications,” Chem. Rev. 108, 2064–2110 (2008). https://doi.org/10.1021/cr068445e

N. Ashrafi, A.H.M. Ariff, M. Sarraf, S. Sulaiman, and T. Hong, “Microstructural, thermal, electrical, and magnetic properties ofoptimized Fe3O4–SiC hybrid nano filler reinforced aluminium matrix composite,” Mater. Chem. Phys. 258, 123895 (2021). https://doi.org/10.1016/j.matchemphys.2020.123895

S. Mokhosi, W. Mdlalose, S. Mngadi, M. Singh, and T. Moyo, “Assessing the structural, morphological and magnetic properties of polymer-coated magnesium-doped cobalt ferrite (CoFe2O4) nanoparticles for biomedical application,” Journal of Physics: Conference Series, 1310, 012014 (2019). https://doi.org/10.1088/1742-6596/1310/1/012014

K.K. Kefeni, and B.B. Mamba, “Photocatalytic application of spinel ferrite nanoparticles and nanocomposites in wastewater treatment,” Sustainable materials and technologies, 23, e00140 (2020). https://doi.org/10.1016/j.susmat.2019.e00140

D.H.K. Reddy, and Y.-S. Yun, “Spinel ferrite magnetic adsorbents: alternative future materials for water purification?” Coord. Chem. Rev. 315, 90–111 (2016). https://doi.org/10.1016/j.ccr.2016.01.012

P.N. Reddy, B.V. Kavyateja, and B.B. Jindal, “Structural health monitoring methods, dispersion of fibers, micro and macro structural properties, sensing, and mechanical properties of self-sensing concrete – A review,” Struct. Concr. 22, 793–805 (2021). https://doi.org/10.1002/suco.202000337

H. Moradmard, S.F. Shayesteh, P. Tohidi, Z. Abbas, and M. Khaleghi, “Structural, magnetic and dielectric properties of magnesium doped nickel ferrite nanoparticles,” J. Alloys Compd. 650, 116–122 (2015). https://doi.org/10.1016/j.jallcom.2015.07.269

J. Xu, H. Yang, W. Fu, K. Du, Y. Sui, J. Chen, Y. Zeng, et al., “Preparation and magnetic properties of magnetite nanoparticles by sol–gel method,” J. Magn. Magn. Mater. 309(2), 307–311 (2007). https://doi.org/10.1016/j.jmmm.2006.07.037

M.D. Hossain, M.A. Hossain, M.S. Hossain, M.N.I. Khan, and S.S. Sikder, “Sintering temperature dependent characterization of Ni nano ferrite with the optimization of frequency dependent properties,” Surf. Interfaces, 52, 104952 (2024). https://doi.org/10.1016/j.surfin.2024.104952

E. Fitriyanti, and B. Purnama, “Comparison XRD pattern of CoFe2O4 thin films and nanoparticles,” J. Phys. Conf. Ser. 909(1), 012010 (2017). https://doi.org/10.1088/1742-6596/909/1/012010

D. Jiao, K. Lesage, M.Y. Yardimci, K. El Cheikh, C. Shi, and G. De Schutter, “Rheological behavior of cement paste with nano-Fe3O4 under magnetic field: Magneto-rheological responses and conceptual calculations,” Cem. Concr. Compos. 120, 104035 (2021). https://doi.org/10.1016/j.cemconcomp.2021.104035

Published
2025-12-08
Cited
How to Cite
Kuvandikov, O., & Nurimov, U. (2025). Production of Magnetic Nanoparticle-Based Ferrites and Comprehensive Characterization of Their Electrical and Magnetic Properties in Colloidal Systems. East European Journal of Physics, (4), 646-650. https://doi.org/10.26565/2312-4334-2025-4-69